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La synthse A est la suivante : 6,72 g de poudre de fer mtallique (Riedel-de Han, 99%), 64 mL d'eau dionise et 33,6 mL d'acide perchlorique 70 % dans l'eau (Riedel-de Han) sont mlangs sous agitation magntique et chauffs 50 0 C pendant 3 heures

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